HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → 9,10-Anthracenedione, 1,5-bis(octadecylamino)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | 1,5-Dichloroanthraquinone | HCID 6711 | — |
| Reactant | Octadecylamine | HCID 15793 | — |
| Reactant | Sodium Acetate | HCID 517045 | — |
| Catalyst | Cupric acetate | HCID 8895 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 9,10-Anthracenedione, 1,5-bis(octadecylamino)- | HCID 3098074 | — |
Reaction Steps
A reactor was charged with 1.4 g of 1, 5-dichloroanthraquinone, 33.6 g. of stearyl amine, 1.3 g of sodium acetate, 0.3 g of copper acetate and 3.2 g of pyridine and the reaction was effected at 80° C. for 15 hours under stirring. The resulting red solid was dissolved in benzene and insoluble matters were removed, followed by distillation of benzene and recystallization from glacial acetic acid. Thus 1, 5-di-n-octadecylaminoanthraquinone was obtained by the reaction of the following formula: ##STR7## Preparation of Liquid Developer:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04051052 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-a0feefa5c5314e0fa83208be9fb5c82c |
| Source note | uspto-grants-1977_09 |