HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1-Dichloroethane → HCID 21525865, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1-Dichloroethane | HCID 6365 | — |
| Reactant | Ethyl aminomalonate hydrochloride | HCID 20464734 | — |
| Reactant | HCID 21407692 | HCID 21407692 | — |
| Product | HCID 21525865 | HCID 21525865 | — |
Reaction Steps
16 g of dry ethyl amino-malonate hydrochloride are suspended in 200 ml of dichloroethane, then a solution of 10 g of 1-phenyl-1-(2-amino-5-chloro-phenyl)-2,5-diazapent-1-ene in 100 ml of dichloroethane is added and the whole is heated at 80° for 3 hours 30 minutes. The red colour at the start changes to yellow at the end of the reaction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04051127 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-66cb38be7b194862829f43ff05c9b00e |
| Source note | uspto-grants-1977_09 |