HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenacyl bromide → 2-Chloro-5-(2-oxo-2-phenylethyl)-5H-thieno[3,2-c]pyridin-1-ium bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenacyl bromide | HCID 6259 | — |
| Reactant | 2-Chlorothieno[3,2-c]pyridine | HCID 598192 | — |
| Product | 2-Chloro-5-(2-oxo-2-phenylethyl)-5H-thieno[3,2-c]pyridin-1-ium bromide | HCID 3041317 | 80.1% |
Reaction Steps
Reaction of 2-chloro-thieno[3,2-c]pyridine (17 g) with phenacyl bromide (20 g) according to the procedure of Example 1 gives white crystals (29.60 g) having a melting point (Koefler block) of 239° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04051141 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-a4de3f34de3145008bccd62ca0a6c15f |
| Source note | uspto-grants-1977_09 |