HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → HCID 22769959, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | p-Toluenesulfonic acid monohydrate | HCID 521998 | — |
| Reactant | HCID 22769962 | HCID 22769962 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 22769959 | HCID 22769959 | — |
Reaction Steps
The crude 3-carboethoxy-2-methylpyr-4-one isolated from the previous reaction is dissolved in 50 ml toluene. 2.4 g of aniline and 400 mg of p-toluenesulfonic acid monohydrate are added and the mixture refluxed for one hour. Evaporation of the solvent leaves 6.3 g of crude 3-carboethoxy-N-phenyl-2-methylpyrid-4-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04051142 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-7033cb2002114fc49fcea616fb9a37bf |
| Source note | uspto-grants-1977_09 |