HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,2',4,4'-Tetrahydroxybenzophenone → 2,2',4,4'-Tetrahydroxybenzophenone beta-(3,4-epoxycyclohexyl)ethyltrimethoxysilane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,2',4,4'-Tetrahydroxybenzophenone | HCID 8571 | — |
| Reactant | Epoxycyclohexylethyltrimethoxysilane | HCID 18819 | — |
| Catalyst | Tetramethylammonium chloride | HCID 6379 | — |
| Product | 2,2',4,4'-Tetrahydroxybenzophenone beta-(3,4-epoxycyclohexyl)ethyltrimethoxysilane | HCID 86735101 | — |
Reaction Steps
The above Adduct III was prepared by heating 2,2',4,4'-tetrahydroxybenzophenone (4.92 g, 0.02 mole) at 80° C with 9.84 g (0.04 mole) of β-(3,4-epoxycyclohexyl)ethyltrimethoxysilane and 0.1 g of tetramethylammonium chloride. A pale, reddish-brown, viscous oil was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04051161 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-6f0fd5d6e4c24ace86acc5b86619cbc6 |
| Source note | uspto-grants-1977_09 |