HuagongsheHuagongshe Chemistry Print Report · For research reference only
Citronellal → Rac.-1-benzyloxy-2,6,10-trimethyl-9-undecen-4-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Citronellal | HCID 7794 | — |
| Reactant | ((3-Bromo-2-methylpropoxy)methyl)benzene | HCID 2735492 | — |
| Product | Rac.-1-benzyloxy-2,6,10-trimethyl-9-undecen-4-ol | HCID 20349060 | — |
Reaction Steps
This compound was prepared starting from the rac. 3-benzyloxy-2-methyl-1-propyl bromide and racemic citronellal using the procedure described in Example 4. Rac.-1-benzyloxy-2,6,10-trimethyl-9-undecen-4-ol was obtained as a colorless oil, b.p. 145°-150° C. (bath temperature) (0.01 mm Hg.)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04051153 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-699971ed35474992834e93e37fb79fd4 |
| Source note | uspto-grants-1977_09 |