HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isobutylene → Rac.-methyl 3-tert. butoxy-2-methylpropionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isobutylene | HCID 8255 | — |
| Reactant | Methyl 3-hydroxy-2-methylpropanoate | HCID 521128 | — |
| Product | Rac.-methyl 3-tert. butoxy-2-methylpropionate | HCID 12923318 | 43.5% |
Reaction Steps
Treatment of rac. methyl-3-hydroxy-2-methylpropionate with isobutylene using the procedure described in Example 1 gave rac.-methyl 3-tert. butoxy-2-methylpropionate in 43.5% yield as a colorless liquid, b.p. 75°-85° C. (bath temperature) (11 mm Hg.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04051153 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-2464328558f9444483179adac7783dcb |
| Source note | uspto-grants-1977_09 |