HRID2072371
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
A mixture of 1-benzoyl-3-(1,2,3,4-tetrahydro-4-oxo- 1-naphthyl)urea (3.8 g) and aqueous sodium hydroxide (2N; 38 ml) is stirred and heated at reflux for 70 minutes. The mixture is then cooled in ice and the product is collected and washed with water to afford 1.83 g of the title compound, m.p. 212° to 215° C.
WORKUP
后处理
- temperatureheated
- temperatureat reflux for 70 minutes
- temperatureThe mixture is then cooled in ice
- customthe product is collected
- washwashed with water