HRID2072371

反应详情

EQUATION

反应方程式

HRID 2072371 的结构方程式

PROCEDURE

实验过程

A mixture of 1-benzoyl-3-(1,2,3,4-tetrahydro-4-oxo- 1-naphthyl)urea (3.8 g) and aqueous sodium hydroxide (2N; 38 ml) is stirred and heated at reflux for 70 minutes. The mixture is then cooled in ice and the product is collected and washed with water to afford 1.83 g of the title compound, m.p. 212° to 215° C.

WORKUP

后处理

  1. temperatureheated
  2. temperatureat reflux for 70 minutes
  3. temperatureThe mixture is then cooled in ice
  4. customthe product is collected
  5. washwashed with water