HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53887742, compound → 3-Amino-4-chloroindazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53887742 | HCID 53887742 | — |
| Solvent | Diethyl Pyrocarbonate | HCID 3051 | — |
| Product | 3-Amino-4-chloroindazole | HCID 313444 | — |
Reaction Steps
Analogously to Example 1, 0.2 mol of 3-amino-4-chloroindazole in 100 ml of pyrocarbonic acid diethyl ester gives 3-amino-4-chloroindazole-2-carboxylic acid ethyl ester (melting point: 109°-111° C; 63% of theory) in 3 hours at 20°-30° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04051252 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-4bfef3b3d31a4d5592e8224df3caf8a3 |
| Source note | uspto-grants-1977_09 |