HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54517551, compound → HCID 21409154, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54517551 | HCID 54517551 | — |
| Solvent | Diethyl Pyrocarbonate | HCID 3051 | — |
| Product | HCID 21409154 | HCID 21409154 | — |
Reaction Steps
Analogously to Example 1, 0.1 mol of 3.7-diamino-5-trifluoromethylindazole in 70 ml of pyrocarbonic acid diethyl ester gives 3,7-diamino-5-trifluoromethylindazole-2-carboxylic acid ethyl ester (melting point: 193°-194° C; 90% of theory) in 1 hour at 20°-30° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04051252 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-01a1b8c1d2e74c9fa25b4ad6eeac7f83 |
| Source note | uspto-grants-1977_09 |