Aminomatacil → HCID 21409290, compound

HRID 2072431Notes

Reaction equation

HRID 2072431 reaction equation
[CH3:1][NH:2][C:3](=[O:13])[O:4][C:5]1[CH:10]=[CH:9][C:8]([NH2:11])=[C:7]([CH3:12])[CH:6]=1.[Cl:14][CH2:15][CH2:16][C:17](Cl)=[O:18]>>[CH3:1][NH:2][C:3](=[O:13])[O:4][C:5]1[CH:10]=[CH:9][C:8]([NH:11][C:17](=[O:18])[CH2:16][CH2:15][Cl:14])=[C:7]([CH3:12])[CH:6]=1

Participants

3

Reactant 2

HCID 25072AminomatacilHCID 693643-Chloropropionyl chloride

Product 1

HCID 21409290HCID 21409290, compound

Procedure

According to the general directions described in Example 5, 3-methyl-4-aminophenyl N-methylcarbamate (1.8g., 0.01 mole) was reacted with 3-chloropropionyl chloride (1.52 g., 0.012 mole). The product weighed 2.0g. after recrystallization from ethanol-water and its infrared spectrum showed a double carbonyl absorption at about 5.8 μ and 6.0 μ.

Workup

  1. customafter recrystallization from ethanol-water and its infrared spectrum
  2. customa double carbonyl absorption at about 5.8 μ and 6.0 μ

Sources & evidence

ORD record
ord-e00e99976f1247cf8273b4e9ed2c3047
Source dataset
uspto-grants-1977_09
Patent number
US04051254

Reaction notes

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