Aminozectran → HCID 53877092, compound

HRID 2072438Notes

Reaction equation

HRID 2072438 reaction equation
[CH3:1][NH:2][C:3](=[O:14])[O:4][C:5]1[CH:10]=[C:9]([CH3:11])[C:8]([NH2:12])=[C:7]([CH3:13])[CH:6]=1.[CH2:15]([S:18](Cl)(=[O:20])=[O:19])[CH2:16][CH3:17]>N1C=CC=CC=1>[CH3:1][NH:2][C:3](=[O:14])[O:4][C:5]1[CH:10]=[C:9]([CH3:11])[C:8]([NH:12][S:18]([CH2:15][CH2:16][CH3:17])(=[O:20])=[O:19])=[C:7]([CH3:13])[CH:6]=1

Participants

4

Reactant 2

HCID 13252AminozectranHCID 662791-Propanesulfonyl chloride

Product 1

HCID 53877092HCID 53877092, compound

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

Following the procedure of Example 22, 3,5-dimethyl-4-aminophenyl N-methylcarbamate (0.8g., 0.004 mole) was reacted with n-propanesulfonyl chloride (0.60g., 0.0042 mole) in pyridine. The product (0.8g.) melted at 173°-76° C.

Sources & evidence

ORD record
ord-e910ced074ec4eef88f133fc41287ad0
Source dataset
uspto-grants-1977_09
Patent number
US04051254

Reaction notes

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