Propargyl bromide → HCID 54296466, compound

HRID 2072528Notes

Reaction equation

[CH3:1][CH:2]([O:10][C:11]1[CH:19]=[CH:18][C:14]([C:15]([OH:17])=[O:16])=[CH:13][CH:12]=1)[CH2:3][CH2:4][CH:5]([CH3:9])[CH:6]([CH3:8])[CH3:7].[CH2:20](Br)[C:21]#[CH:22]>>[CH2:22]([O:16][C:15](=[O:17])[C:14]1[CH:18]=[CH:19][C:11]([O:10][CH:2]([CH3:1])[CH2:3][CH2:4][CH:5]([CH3:9])[CH:6]([CH3:7])[CH3:8])=[CH:12][CH:13]=1)[C:21]#[CH:20]

Participants

Reactant 2

HCID 7842Propargyl bromide

HCID 22749287HCID 22749287, compound

Product 1

HCID 54296466HCID 54296466, compound

Procedure

By utilizing th procedure of Example 8, by reacting p-[(1,4,5-trimethylhexyl)oxy]benzoic acid with propargyl bromide, there is obtained p-[(1,4,5-trimethylhexyl)oxy]benzoic acid propargyl ester; nD22 = 1.5050.

Sources & evidence

ORD record: ord-588d0b3a375145feb7623cbd40a2ea82
Source dataset: uspto-grants-1977_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04051319

Reaction notes

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