HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propargyl alcohol → p-[(1,5-Dimethylhexyl)oxy]benzoic acid propargyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propargyl alcohol | HCID 7859 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 54404637 | HCID 54404637 | — |
| Product | p-[(1,5-Dimethylhexyl)oxy]benzoic acid propargyl ester | HCID 53978508 | — |
Reaction Steps
10 g of p-[(1,5-dimethylhexyl)oxy]benzoic acid methyl ester, 30 of propargyl alcohol and 0.5 g of sodium methoxide are heated to reflux for 1/2 an hour The excess propargyl alcohol is thereupon slowly (5 hrs.) distilled off. The residue is poured onto water and extracted with diethyl ether. The ether solution is dried with sodium sulfate and evaporated. The dark-yellow p-[(1,5-dimethylhexyl)oxy]benzoic acid propargyl ester obtained is purified over Kieselgel.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04051319 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-c4355eae54ec40aabf2e39451f28419e |
| Source note | uspto-grants-1977_09 |