Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Phenylphenol → Methyl(3-phenylphenoxy)acetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Phenylphenol | HCID 11381 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | Methyl bromoacetate | HCID 60984 | — |
| 용매 | Water | HCID 962 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | Methyl(3-phenylphenoxy)acetate | HCID 13787157 | — |
반응 단계
A mixture of 3-phenylphenol (5.00 g), methyl bromoacetate (3.1 ml) and potassium carbonate (8.1 g) in DMF was stirred at room temperature. After five hours, the reaction mixture was diluted with water (100 ml) and then extracted with ether. The combined organic layers were washed with aqueous sodium carbonate followed by brine and then dried, filtered and evaporated to give crude methyl (3-phenylphenoxy)acetate (7.2 g) as a pale yellow liquid, 1H NMR (CDCl3) delta 3.8 (3H,s), 4.7 (2H,s), 6.8-7.6 (9H,m) ppm.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04913721 |
| 출처 데이터셋 | uspto-grants-1990_04 |
| ORD ID | ord-305bc901054e41edb770689a8a579347 |
| 출처 메모 | uspto-grants-1990_04 |