HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 3-Bromo-4-(2'-methylbutyl)benzoic acid chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 3-Bromo-4-(2'-methylbutyl)benzoic acid | HCID 19859966 | — |
| Product | 3-Bromo-4-(2'-methylbutyl)benzoic acid chloride | HCID 53842980 | 98.1% |
Reaction Steps
Thionyl chloride (118 g) was added to the 3-bromo-4-(2'-methylbutyl)benzoic acid (100 g, 0.37 mol) followed by refluxing the mixture for 2 hours and distilling off excess thionyl chloride under reduced pressure to obtain 3-bromo-4-(2'-methylbutyl)benzoic acid chloride (105.1 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04913838 |
| Source dataset | uspto-grants-1990_04 |
| ORD ID | ord-7960b18b5e314dc7a1ced42d775b266e |
| Source note | uspto-grants-1990_04 |