HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → Ethyl 4'-hydroxy-4-biphenylcarboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 4'-Hydroxy-4-biphenylcarboxylic acid | HCID 301556 | — |
| Product | Ethyl 4'-hydroxy-4-biphenylcarboxylate | HCID 4049156 | 97% |
Reaction Steps
1 ml of conc. sulfuric acid was added to an ethanol solution of 0.1 mole (21.4 g) of 4'-hydroxybiphenyl-4-carboxylic acid, and stirred for 18 hours. The reaction solution was concentrated, and then purified by column chromatography, to obtain 22.8 g of 4'-hydroxybiphenyl-4-carboxylic acid ethyl ester [m.p. 144.4°-145.6° C⟧ (yield: 97%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04913839 |
| Source dataset | uspto-grants-1990_04 |
| ORD ID | ord-31ca842f45f34d8a85394ca307d3f903 |
| Source note | uspto-grants-1990_04 |