HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → 4'-(12-Hydroxydodecyloxy)biphenyl-4-carboxylic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 4'-(12-Acetyloxydodecyloxy)biphenyl-4-carboxylic acid ethyl ester | HCID 53656928 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Water | HCID 962 | — |
| Product | 4'-(12-Hydroxydodecyloxy)biphenyl-4-carboxylic acid | HCID 19779581 | 98% |
Reaction Steps
30 m moles (14.1 g) of the above 4'-(12-acetyloxydodecyloxy)biphenyl-4-carboxylic acid ethyl ester and 10 g of sodium hydroxide were stirred for 10 min. at 70° C. in 40 ml of ethanol and 80 ml of water. After the reaction, the reaction solution was concentrated to obtain 11.7 g of 4'-(12-hydroxydodecyloxy)biphenyl-4-carboxylic acid. (yield: 98%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04913839 |
| Source dataset | uspto-grants-1990_04 |
| ORD ID | ord-e0d16f4eeaa54cbe849629fbaa79d91b |
| Source note | uspto-grants-1990_04 |