Thionyl Chloride → HCID 14499651, compound

HRID 2072664Notes

Reaction equation

HRID 2072664 reaction equation
[O:1]=[C:2]([N:9]1[CH2:15][CH2:14][CH2:13][CH2:12][CH2:11][CH2:10]1)[CH2:3][N:4]([CH3:8])[CH2:5][CH2:6]O.S(Cl)([Cl:18])=O>C(Cl)(Cl)Cl>[Cl:18][CH2:6][CH2:5][N:4]([CH3:8])[CH2:3][C:2](=[O:1])[N:9]1[CH2:15][CH2:14][CH2:13][CH2:12][CH2:11][CH2:10]1

Participants

4

Reactant 2

HCID 24386Thionyl ChlorideHCID 14499650HCID 14499650, compound

Product 1

HCID 14499651HCID 14499651, compound

Reagents, catalysts & solvents 1

HCID 6212ChloroformSolvent

Procedure

A mixture of 5.7 g (27 mmol) of 2-{N-[2-oxo-2- (perhydro-1-azepinyl) ethyl]methylamino}ethanol, dissolved in 50 ml of chloroform, and 6 ml (excess) of thionyl chloride is heated under reflux for 2 h.

Workup

  1. temperatureunder reflux for 2 h.

Sources & evidence

ORD record
ord-974e2862fa544b97bb49f6c8e4c548f0
Source dataset
uspto-grants-1990_04
Patent number
US04914092

Reaction notes

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