(Dimethyl sulfide)trihydroboron → HCID 19860369, compound

HRID 2072774Notes

Reaction equation

HRID 2072774 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH:8]2[O:13][CH2:12][C:11](=O)[N:10]([CH:15]([CH3:17])[CH3:16])[CH2:9]2)[CH:5]=[CH:6][CH:7]=1.B.CSC>CO.C(OCC)(=O)C>[ClH:1].[Cl:1][C:2]1[CH:3]=[C:4]([CH:8]2[O:13][CH2:12][CH2:11][N:10]([CH:15]([CH3:17])[CH3:16])[CH2:9]2)[CH:5]=[CH:6][CH:7]=1

Participants

4

Reactant 2

HCID 12423031(Dimethyl sulfide)trihydroboronHCID 19913610HCID 19913610, compound

Product 1

HCID 19860369HCID 19860369, compound

Reagents, catalysts & solvents 1

HCID 21584119Ethylacetate methanolSolvent

Procedure

The title compound, m.p. 224°-5° C. (methanol-ethyl acetate), was prepared from 2-[3-chlorophenyl]-4-[1-methylethyl]-5-oxomorpholine and borane-methyl sulphide by an analogous procedure to that described in Example 1.

Sources & evidence

ORD record
ord-8f1f0c7c6fab4a8a893838d2456c707d
Source dataset
uspto-grants-1990_04
Patent number
US04914202

Reaction notes

Loading…