(Dimethyl sulfide)trihydroboron → HCID 19860372, compound

HRID 2072775Notes

Reaction equation

HRID 2072775 reaction equation
[NH2:1][C:2]1[C:7]([Cl:8])=[CH:6][C:5]([CH:9]2[O:14][CH2:13][C:12](=O)[N:11]([C:16]([CH3:19])([CH3:18])[CH3:17])[CH2:10]2)=[CH:4][C:3]=1[Cl:20].B.CSC>>[ClH:8].[NH2:1][C:2]1[C:3]([Cl:20])=[CH:4][C:5]([CH:9]2[O:14][CH2:13][CH2:12][N:11]([C:16]([CH3:18])([CH3:17])[CH3:19])[CH2:10]2)=[CH:6][C:7]=1[Cl:8]

Participants

3

Reactant 2

HCID 12423031(Dimethyl sulfide)trihydroboronHCID 19913617HCID 19913617, compound

Product 1

HCID 19860372HCID 19860372, compound

Procedure

The title compound, m.p. 283°-4° C. (d) (methanol-ethyl acetate), was prepared from 2-[4-amino-3,5-dichlorophenyl]-4-[1,1-dimethylethyl]-5-oxo morpholine and borane-methyl sulphide by an analogous procedure to that described in Example 1.

Sources & evidence

ORD record
ord-42a0df307b2d4a7db521e8b29ef08aa1
Source dataset
uspto-grants-1990_04
Patent number
US04914202

Reaction notes

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