HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 14390325, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | HCID 15617195 | HCID 15617195 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 14390325 | HCID 14390325 | — |
Reaction Steps
Under nitrogen bubbling, a mixture of 2-(4-methoxyphenyl-3H-imidazo[4,5-b]pyridine-3-acetic acid (4.2 g, 0.0148 mole) and 1,1'-carbonyldiimidazole (2.43 g, 0.015 mole) in 120 ml of tetrahydrofuran was stirred at room temperature for 31/2 hrs. A solution of dimethylamine in tetrahydrofuran (60 ml of 0.5M) was added, and the reaction was allowed to stir at room temperature overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04914109 |
| Source dataset | uspto-grants-1990_04 |
| ORD ID | ord-a78f71db4f9045b7afb57d3e8566a68b |
| Source note | uspto-grants-1990_04 |