7-Diethylaminoheptylamine → HCID 20073311, compound

HRID 2073290Notes

Reaction equation

HRID 2073290 reaction equation
[CH3:1][C:2]1[CH:3]=[C:4]([C:8]2[CH:9]=[N:10][N:11]([CH2:19][C:20]([NH2:22])=[O:21])[C:12]=2[C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[CH:5]=[CH:6][CH:7]=1.[CH2:23]([N:25]([CH2:34][CH3:35])[CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32]N)[CH3:24].CC1C=C(C2C=NN(CC(OCC)=O)C=2C2C=CC=CC=2)C=CC=1.CC1C=C(CC(C2C=CC=CC=2)=O)C=CC=1>>[CH2:34]([N:25]([CH2:23][CH3:24])[CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][NH:22][C:20](=[O:21])[CH2:19][N:11]1[C:12]([C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=[C:8]([C:4]2[CH:5]=[CH:6][CH:7]=[C:2]([CH3:1])[CH:3]=2)[CH:9]=[N:10]1)[CH3:35]

Participants

5

Reactant 4

HCID 37094117-DiethylaminoheptylamineHCID 131736142-(3-Methylphenyl)acetophenoneHCID 54470792HCID 54470792, compoundHCID 867434074-(3-methylphenyl)-5-phenyl-1H-pyrazole-1-acetamide

Product 1

HCID 20073311HCID 20073311, compound

Procedure

By a process substantially similar to that of Example 30 it is contemplated that N-7-(diethylamino)heptyl]-4-(3-methylphenyl)-5-phenyl-1H-pyrazole-1-acetamide may be synthesized from N,N-diethyl-1,7-heptanediamine and ethyl 4-(3-methylphenyl)-5-phenyl-1H-pyrazole-1-acetate, which is synthesized by a process substantially similar to that of Example 1B from 2-(3-methylphenyl)-1-phenylethanone.

Sources & evidence

ORD record
ord-502b278acb674069b6b0a536f2f5c429
Source dataset
uspto-grants-1990_04
Patent number
US04916150

Reaction notes

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