HuagongsheHuagongshe Chemistry Print Report · For research reference only
3',4'-Dimethoxy-2-(2-propenyl)-N-[1-methyl-4-(3-pyridinyl)butyl][1,1'-biphenyl]-4-carb oxamide → (R)-3',4'-Dimethoxy-2-propyl-N-[1-methyl-4-(3-Pyridinyl)butyl][1,1'-biphenyl]-4-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3',4'-Dimethoxy-2-(2-propenyl)-N-[1-methyl-4-(3-pyridinyl)butyl][1,1'-biphenyl]-4-carb oxamide | HCID 14570106 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | (R)-3',4'-Dimethoxy-2-propyl-N-[1-methyl-4-(3-Pyridinyl)butyl][1,1'-biphenyl]-4-carboxamide | HCID 14570109 | 94.6% |
Reaction Steps
A solution of 282 mg of 3',4'-Dimethoxy-2-(2-propenyl)-N-[1-methyl-4-(3-pyridinyl)butyl][1,1'-biphenyl]-4-carb oxamide was hydrogenated over 40 mg of 10% palladium on carbon to give 268 mg of (R)-3',4'-Dimethoxy-2-propyl-N-[1-methyl-4-(3-Pyridinyl)butyl][1,1'-biphenyl]-4-carboxamide as a foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04916145 |
| Source dataset | uspto-grants-1990_04 |
| ORD ID | ord-b22dbcb974ff4fa9ba40ce6c6da05aae |
| Source note | uspto-grants-1990_04 |