HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl Peroxide → HCID 19858042, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 19858068 | HCID 19858068 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 19858042 | HCID 19858042 | — |
Reaction Steps
A mixture of 1,1,8-trimethyl-2(1H)-naphtho[2,1-b]furanone (1.13 g), N-bromosuccinimide (0.98 g), benzoyl peroxide (0.05 g) and carbon tetrachloride (30 ml) was heated under reflux for 1.5 h and filtered, and the filtrate was evaporated to dryness under reduced pressure, to give 8-bromomethyl-1,1-dimethyl-2[1H]-naphtho[2,1-b]furanone, which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04916148 |
| Source dataset | uspto-grants-1990_04 |
| ORD ID | ord-0fdf49a8e7d24234862cda40d3dcc5bd |
| Source note | uspto-grants-1990_04 |