HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl Peroxide → HCID 14774132, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | Diethyl 2-(2-methylphenoxy)pentanedioate | HCID 14774131 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 14774132 | HCID 14774132 | — |
Reaction Steps
A mixture of ethyl 4-carbethoxy-4-(2-methylphenoxy)butyrate (0.05 mol) and NBS (0.055 mol) and 150 mg of benzoyl peroxide in 150 mL of CCl4 is refluxed and shined with a sun lamp for 2 hours. Filtration and evaporation of solvent gives 2-(1,3-dicarbethoxypropoxy) benzyl bromide which is used without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04918081 |
| Source dataset | uspto-grants-1990_04 |
| ORD ID | ord-0839f3440f8543c5bb5606b4f47a14ea |
| Source note | uspto-grants-1990_04 |