HCID 14677704, compound → HCID 14677705, compound

Participants

Reaction Steps

The compound of Example 4 (275 mg, 0.61 mmoles) was taken up in approximately 5 ml THF to which was added in NaOH (1.3 ml). After 2 hours, the THF was removed in vacuo and the aqueous phase was diluted with two volumes of distilled H2O acidified with concentrated HCl. The title compound was extracted into CHCl3, dried and concentrated to a beige solid, m.p. 156°-158°

Provenance & Evidence