HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropanol → HCID 19857591, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | Styrene Oxide | HCID 7276 | — |
| Reactant | Cyclohexylhydroxylamine | HCID 72935 | — |
| Product | HCID 19857591 | HCID 19857591 | 33% |
Reaction Steps
A solution of 2.14 g of N-cyclohexylhydroxylamine and 2.23 of styrene oxide in 50 ml of isopropanol is heated at 45° C. for 3 hours and under reflux for 20 hours. The reaction mixture is concentrated under reduced pressure and the residue is purified by liquid chromatography to afford the title compound in a 33% yield as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04918189 |
| Source dataset | uspto-grants-1990_04 |
| ORD ID | ord-d9f30f768b6446feb4550fe953e3f287 |
| Source note | uspto-grants-1990_04 |