HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 2-(3-nitrobenzylidene)-3-oxobutanoate → HCID 2790872, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 2-(3-nitrobenzylidene)-3-oxobutanoate | HCID 367507 | — |
| Reactant | HCID 178509299 | HCID 178509299 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 2790872 | HCID 2790872 | 61.3% |
Reaction Steps
To 50 ml of ethanol are added 2.6 g of ethyl 3-nitro-α-acetylcinnamate and 0.9 g of 5-aminotetrazole, and then heated under reflux for 16 hours. On cooling, 2 g of 6-ethoxycarbonyl-5-methyl-7-(3-nitrophenyl)-4,7-dihydrotetrazolo[1,5-a]pyrimidine, melting at 210°-212° C., is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04918074 |
| Source dataset | uspto-grants-1990_04 |
| ORD ID | ord-ba395cf0e45848e388795a40ef3449b9 |
| Source note | uspto-grants-1990_04 |