HCID 19855950, compound → HCID 19855928, compound

HRID 2073728Notes

Reaction equation

HRID 2073728 reaction equation
[CH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[CH:11]([CH2:14][N:15]1[CH2:20][CH2:19][N:18]([CH2:21][CH2:22][CH2:23][CH2:24][CH3:25])[CH2:17][CH2:16]1)[C:12]#[N:13].[H-].[Al+3].[Li+].[H-].[H-].[H-]>>[CH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[CH:11]([CH2:14][N:15]1[CH2:20][CH2:19][N:18]([CH2:21][CH2:22][CH2:23][CH2:24][CH3:25])[CH2:17][CH2:16]1)[CH2:12][NH2:13]

Participants

3

Reactant 2

HCID 19855950HCID 19855950, compoundHCID 21226445Aluminium lithium hydride

Product 1

HCID 19855928HCID 19855928, compound

Procedure

In a manner similar to Preparation 2 react α-(2-naphthalenyl)-4-pentylpiperazinepropanenitrile with lithium aluminum hydride to obtain the title compound.

Workup

  1. customIn a manner similar to Preparation 2

Sources & evidence

ORD record
ord-a7e2d03e1da549038e875122479f9246
Source dataset
uspto-grants-1990_04
Patent number
US04920116

Reaction notes

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