HCID 19855901, compound → HCID 19855895, compound

HRID 2073729Notes

Reaction equation

HRID 2073729 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([NH:10][C:11](=O)[CH2:12][N:13]([CH2:21][CH3:22])[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20])[CH:5]=[CH:6][C:7]=1[O:8][CH3:9].[H-].[Al+3].[Li+].[H-].[H-].[H-]>>[Cl:1][C:2]1[CH:3]=[C:4]([NH:10][CH2:11][CH2:12][N:13]([CH2:21][CH3:22])[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20])[CH:5]=[CH:6][C:7]=1[O:8][CH3:9]

Participants

3

Reactant 2

HCID 19855901HCID 19855901, compoundHCID 21226445Aluminium lithium hydride

Product 1

HCID 19855895HCID 19855895, compound

Procedure

In a manner similar to Preparation 2 react N-(3-chloro-4-methoxyphenyl)-2-[ethyl(heptyl)amino]acetamide with lithium aluminum hydride to obtain the title compound.

Workup

  1. customIn a manner similar to Preparation 2

Sources & evidence

ORD record
ord-336c748773a84cc48d7dfaa3322a2aa4
Source dataset
uspto-grants-1990_04
Patent number
US04920116

Reaction notes

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