HCID 19855933, compound → HCID 19855920, compound

HRID 2073732Notes

Reaction equation

HRID 2073732 reaction equation
[Cl:1][C:2]1[CH:7]=[C:6]([O:8][CH3:9])[CH:5]=[CH:4][C:3]=1[NH:10][C:11](=O)[CH2:12][N:13]([CH2:17][CH:18]1[CH2:23][CH2:22][CH2:21][CH2:20][CH2:19]1)[CH2:14][CH:15]=[CH2:16].[H-].[Al+3].[Li+].[H-].[H-].[H-]>>[Cl:1][C:2]1[CH:7]=[C:6]([O:8][CH3:9])[CH:5]=[CH:4][C:3]=1[NH:10][CH2:11][CH2:12][N:13]([CH2:17][CH:18]1[CH2:19][CH2:20][CH2:21][CH2:22][CH2:23]1)[CH2:14][CH:15]=[CH2:16]

Participants

3

Reactant 2

HCID 19855933HCID 19855933, compoundHCID 21226445Aluminium lithium hydride

Product 1

HCID 19855920HCID 19855920, compound

Procedure

In a manner similar to Preparation 2 react N-(2-chloro-4-methoxyphenyl)-2-[cyclohexylmethyl(2-propenyl)-amino]acetamide with lithium aluminum hydride to obtain the title compound.

Workup

  1. customIn a manner similar to Preparation 2

Sources & evidence

ORD record
ord-1dff0a6cd0d043769e44f013c8ff152f
Source dataset
uspto-grants-1990_04
Patent number
US04920116

Reaction notes

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