HCID 19855924, compound → HCID 19855957, compound

HRID 2073736Notes

Reaction equation

HRID 2073736 reaction equation
[CH2:1]([O:5][C:6]1[CH:11]=[CH:10][C:9]([NH:12][C:13](=O)[CH2:14][CH2:15][N:16]([CH2:18][CH2:19][C:20]2[CH:25]=[CH:24][C:23]([O:26][CH3:27])=[C:22]([O:28][CH3:29])[CH:21]=2)[CH3:17])=[CH:8][CH:7]=1)[CH2:2][CH2:3][CH3:4].[H-].[Al+3].[Li+].[H-].[H-].[H-]>>[CH2:1]([O:5][C:6]1[CH:7]=[CH:8][C:9]([NH:12][CH2:13][CH2:14][CH2:15][N:16]([CH2:18][CH2:19][C:20]2[CH:25]=[CH:24][C:23]([O:26][CH3:27])=[C:22]([O:28][CH3:29])[CH:21]=2)[CH3:17])=[CH:10][CH:11]=1)[CH2:2][CH2:3][CH3:4]

Participants

3

Reactant 2

HCID 19855924HCID 19855924, compoundHCID 21226445Aluminium lithium hydride

Product 1

HCID 19855957HCID 19855957, compound

Procedure

In a manner similar to Preparation 2 react N-[4-butoxyphenyl]-3-[[2-(3,4-dimethoxyphenyl)ethyl](methyl)amino]propionamide with lithium aluminum hydride to obtain the title compound.

Workup

  1. customIn a manner similar to Preparation 2

Sources & evidence

ORD record
ord-3de294df44b845be96fa709ac3f81c43
Source dataset
uspto-grants-1990_04
Patent number
US04920116

Reaction notes

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