3',4',5'-Trimethoxyacetophenone → 2-Bromo-1-(3,4,5-trimethoxyphenyl)ethanone

HRID 2073741Notes

Reaction equation

HRID 2073741 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([C:13](=[O:15])[CH3:14])[CH:6]=[C:7]([O:11][CH3:12])[C:8]=1[O:9][CH3:10].[Br:16]Br>>[Br:16][CH2:14][C:13]([C:5]1[CH:6]=[C:7]([O:11][CH3:12])[C:8]([O:9][CH3:10])=[C:3]([O:2][CH3:1])[CH:4]=1)=[O:15]

Participants

3

Reactant 2

HCID 143453',4',5'-TrimethoxyacetophenoneHCID 24408Bromine

Product 1

HCID 36857322-Bromo-1-(3,4,5-trimethoxyphenyl)ethanone

Procedure

In a manner similar to Preparation 30 react 1-(3,4,5-trimethoxyphenyl)ethanone with bromine to obtain the title compound.

Workup

  1. customIn a manner similar to Preparation 30

Sources & evidence

ORD record
ord-bb42e8cd60f04102924f647b4ac24331
Source dataset
uspto-grants-1990_04
Patent number
US04920116

Reaction notes

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