Sodium Azide → HCID 19855932, compound

HRID 2073742Notes

Reaction equation

HRID 2073742 reaction equation
Br[CH2:2][C:3]([C:5]1[CH:10]=[C:9]([O:11][CH3:12])[C:8]([O:13][CH3:14])=[C:7]([O:15][CH3:16])[CH:6]=1)=[O:4].[N-:17]=[N+:18]=[N-:19].[Na+]>>[N:17]([CH2:2][C:3]([C:5]1[CH:10]=[C:9]([O:11][CH3:12])[C:8]([O:13][CH3:14])=[C:7]([O:15][CH3:16])[CH:6]=1)=[O:4])=[N+:18]=[N-:19]

Participants

3

Reactant 2

HCID 33557Sodium AzideHCID 36857322-Bromo-1-(3,4,5-trimethoxyphenyl)ethanone

Product 1

HCID 19855932HCID 19855932, compound

Procedure

In a manner similar to Preparation 3 react 2-bromo-1-(3,4,5-trimethoxyphenyl)ethanone with NaN3 to obtain the title compound.

Workup

  1. customIn a manner similar to Preparation 3

Sources & evidence

ORD record
ord-5c4e8a49aad54bcb9a019b04d30ba6a4
Source dataset
uspto-grants-1990_04
Patent number
US04920116

Reaction notes

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