Thionyl Chloride → HCID 19855917, compound

HRID 2073753Notes

Reaction equation

HRID 2073753 reaction equation
[CH2:1]([S:5]([NH:8][C:9]1[CH:17]=[CH:16][C:12]([C:13](O)=[O:14])=[CH:11][CH:10]=1)(=[O:7])=[O:6])[CH2:2][CH2:3][CH3:4].O=S(Cl)[Cl:20]>>[CH2:1]([S:5]([NH:8][C:9]1[CH:17]=[CH:16][C:12]([C:13]([Cl:20])=[O:14])=[CH:11][CH:10]=1)(=[O:7])=[O:6])[CH2:2][CH2:3][CH3:4]

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 16776736HCID 16776736, compound

Product 1

HCID 19855917HCID 19855917, compound

Procedure

In a manner similar to Preparation 10 react 4-[(1-butylsulfonyl)amino]benzoic acid with SOCl2 to obtain the title compound.

Workup

  1. customIn a manner similar to Preparation 10

Sources & evidence

ORD record
ord-84c4e2bd54b44908b6efcced7b8c4062
Source dataset
uspto-grants-1990_04
Patent number
US04920116

Reaction notes

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