1,2-Ethanediamine, N1,N1-diethyl-N2-phenyl- → N-[2-(Diethylamino)ethyl]-4-[(methylsulfonyl)amino]-N-(phenyl)benzamide hydrochloride
Reaction equation
[CH2:1]([N:3]([CH2:13][CH3:14])[CH2:4][CH2:5][NH:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1)[CH3:2].[CH3:15][S:16]([NH:19][C:20]1[CH:28]=[CH:27][C:23]([C:24]([Cl:26])=[O:25])=[CH:22][CH:21]=1)(=[O:18])=[O:17]>>[ClH:26].[CH2:13]([N:3]([CH2:1][CH3:2])[CH2:4][CH2:5][N:6]([C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1)[C:24](=[O:25])[C:23]1[CH:27]=[CH:28][C:20]([NH:19][S:16]([CH3:15])(=[O:18])=[O:17])=[CH:21][CH:22]=1)[CH3:14]Participants
3
Procedure
In a manner similar to Example I react N,N-diethyl-N'-phenyl-1,2-ethanediamine with 4-[(methylsulfonyl)amino]benzoyl chloride to obtain the title compound.
Sources & evidence
- ORD record
- ord-d6f74fdef47b40c1b1d81d06824fa57e
- Source dataset
- uspto-grants-1990_04
- Patent number
- US04920116
Reaction notes
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