HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → HCID 53869832, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | HCID 19856159 | HCID 19856159 | — |
| Product | HCID 53869832 | HCID 53869832 | — |
Reaction Steps
A solution of 4-(4-(2-quinolinylmethyloxy)benzyl)-benzoyl chloride (0.05 mol) in tetrahydrofuran (300 ml) is added to a concentrated ammonium hydroxide (25 ml) solution and the reaction stirred overnight. The reaction mixture is evaporated and partitioned between ethyl acetate and water. The ethyl acetate fraction is dried and evaporated to give 4-(4-(2-quinolinylmethyloxy)styryl)benzamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04920130 |
| Source dataset | uspto-grants-1990_04 |
| ORD ID | ord-0fd23a8efe2a483882c2e8ca0b0aaa8f |
| Source note | uspto-grants-1990_04 |