HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2073866Generated: November 1, 2026
Diisobutylaluminumhydride → HCID 53915721, compound
https://huagongshe.com/reaction/2073866
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Diisobutylaluminumhydride | HCID 21225700 | — |
| Reactant | HCID 53866563 | HCID 53866563 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 53915721 | HCID 53915721 | — |
Reaction Steps
A solution of diisobutyl aluminum hydride (0.01 mol) in hexane is added dropwise to a solution of methyl 4-(3-(2-quinolinylmethyloxy)styryl)benzoate (0.01 mol) in 100 ml of THF at 0° C. The reaction mixture is stirred at 0° C. got 40 minutes and then quenched with methanol and Rochelle salt. Extraction with ethyl acetate and purified by column chromatography gives 4-(3-(2-quinolinylmethyloxy)styryl)-benzaldehyde.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04920130 |
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| Source dataset | uspto-grants-1990_04 |
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| ORD ID | ord-fd3ac41b567448c7a420d93d7cad07fd |
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| Source note | uspto-grants-1990_04 |
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