Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | HCID 14800671 | HCID 14800671 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178420092 | HCID 178420092 | — |
Reaction Steps
A mixture of sodium azide (0.03 mol), ammonium chloride (0.03 mol) and 3-(4-(2-quinolinylmethyloxy)benzyl)benzonitrile (0.01 mol) in dimethylformamide (20 ml) are heated at 100° C. for 18 hours. The reaction is poured into aqueous 10% sodium hydroxide solution and washed with ethyl acetate. The crystalline product is isolated by acidification and filtration to obtain 5-(3-(4-(2-quinolinylmethyloxy)benzyl)phenyl)tetrazole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04920133 |
|---|
| Source dataset | uspto-grants-1990_04 |
|---|
| ORD ID | ord-21e5f173722f415899fc983e0efc8f79 |
|---|
| Source note | uspto-grants-1990_04 |
|---|
