HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2073885Generated: October 31, 2026
HCID 14800776, compound → HCID 14800777, compound
https://huagongshe.com/reaction/2073885
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 14800776 | HCID 14800776 | — |
| Reactant | Diisobutylaluminumhydride | HCID 21225700 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 14800777 | HCID 14800777 | — |
Reaction Steps
A solution of diisobutyl aluminum hydride (0.01 mol) in hexane is added dropwise to a solution of methyl 3-(3-(2-quinolinylmethyloxy)benzyl)benzoate (0.01 mol) in 100 ml of THF at 0° C. The reaction mixture is stirred at 0° C. for 30 minutes and then quenched with methanol and Rochelle salt. Extraction with ethyl acetate and purified by column chromatography gives 3-(3-(2-quinolinylmethyloxy)benzyl)benzaldehyde.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04920133 |
|---|
| Source dataset | uspto-grants-1990_04 |
|---|
| ORD ID | ord-c78b306d90ae4957ae6397a43bd329c4 |
|---|
| Source note | uspto-grants-1990_04 |
|---|
