HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → HCID 14995012, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | Potassium Bicarbonate | HCID 516893 | — |
| Reactant | HCID 14995011 | HCID 14995011 | — |
| Solvent | 1,2-Dichloroethylene | HCID 10900 | — |
| Product | HCID 14995012 | HCID 14995012 | — |
Reaction Steps
4-(4-(2-quinolinylmethylthio)phenethyl)benzoic acid (4 mmol) in dichloroethene (50 ml) is stirred with m-chloroperbenzoic acid (4 mmol) and solid potassium hydrogen carbonate (1.0 g). The reaction is assayed by TLC and upon consumption of the starting thio compound, the mixture is filtered, washed with dilute aqueous sodium bisulfite, dried and evaporated to give 4-(4-(2-quinolinylmethylsulfinyl)phenethyl)benzoic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04920133 |
| Source dataset | uspto-grants-1990_04 |
| ORD ID | ord-f8af089819b84ca0acde9b41d02aa2a6 |
| Source note | uspto-grants-1990_04 |