2-Methyl-2-butanol → HCID 54165407, compound

Participants

Reaction Conditions

Reaction Steps

Sodium hydride (with 20% of paraffin oil; 2.25 g, 75 mmol) was stirred under reflux with absolute toluene (50 ml) and tert.-amyl alcohol (7.25 g, 82.5 mmol) was added dropwise within 30 minutes. When the solution had cooled to 100° C., 4-(4-chlorophenoxy)-3',4'-dimethoxy benzophenone (9.22 g, 25 mmol) and acetyl morpholine (16.17 g, 125 mmol) were added and the mixture was stirred under reflux for 8 hours.

Provenance & Evidence