HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57507786, compound → HCID 57507787, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57507786 | HCID 57507786 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 57507787 | HCID 57507787 | 78.9% |
Reaction Steps
Pyridin-3-yl 4-({[2-(methylamino)phenyl]amino}carbonyl)piperidine-1-carboxylate (0.41 g) was dissolved in acetic acid (10 ml), followed by heating under reflux for 2 hours. The solvent was evaporated, and the residue was recrystallized from methanol and diethyl ether to obtain (pyridin-3-yl) 4-(1-methyl-1H-benzimidazol-2-yl)piperidine-1-carboxylate (307 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07919495B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-69ec576f3cd5452cbc9b8dcd0741dcd8 |
| Source note | uspto-grants-2011_04 |