Hydrochloride methanol → HCID 67089732, compound

Participants

Reaction Conditions

Reaction Steps

A solution of Compound 82 (100 mg, 0.224 mmol) in methanol (10.0 mL) was added with 10% hydrogen chloride-methanol solution (10.0 mL), followed by stirring at 60° C. for 2 hours. After cooling to room temperature, deposited crystal was collected by filtration to obtain Compound 85 (48.7 mg, 47%).

Provenance & Evidence