HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propylamine hydrochloride → HCID 11695786, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propylamine hydrochloride | HCID 11165 | — |
| Reactant | HCID 76850762 | HCID 76850762 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 11695786 | HCID 11695786 | — |
Reaction Steps
Treat 5-formyl-3-phenylsulfanyl-1H-indole-2-carboxylic acid amide 13 (m=0, R3=Ph) (80 mg, 0.27 mmol) with propylamine hydrochloride (28 mg, 0.30 mmol) as described in General Procedure X to afford Iae (41.0 mg, 44.8%) as an ivory colored solid, tlc Rf=0.1 (10% MeOH/CH2Cl2−0.2% Et3N), m/z obs=340 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07923466B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-31d7180a69894a36a776dd7c31305e0b |
| Source note | uspto-grants-2011_04 |