HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Aminopropanamide → HCID 11703390, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Aminopropanamide | HCID 350287 | — |
| Reactant | HCID 76850762 | HCID 76850762 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 11703390 | HCID 11703390 | — |
Reaction Steps
Treat 5-formyl-3-phenylsulfanyl-1H-indole-2-carboxylic acid amide 13 (m=0, R3=Ph) (50 mg, 0.17 mmol) with 2-aminopropionamide (62.3 mg, 0.50 mmol) as described in General Procedure X to afford Iaf (39 mg, 62.9%) as an ivory colored solid, tlc Rf=0.5 (10% MeOH/CH2Cl2−0.2% Et3N), m/z obs=369 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07923466B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-cd91ce3590a549a2afe0705b55c17714 |
| Source note | uspto-grants-2011_04 |