HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Butylaniline → HCID 11590033, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Butylaniline | HCID 7694 | — |
| Reactant | HCID 76850762 | HCID 76850762 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 11590033 | HCID 11590033 | — |
Reaction Steps
Treat 5-formyl-3-phenylsulfanyl-1H-indole-2-carboxylic acid amide 13 (m=0, R3=Ph) (50 mg, 0.17 mmol) with 4-butylaniline (74 mg, 0.50 mmol) as described in General Procedure X to afford Iah (17 mg, 23.4%) as an ivory colored solid, tlc Rf=0.8 (5% MeOH/CH2Cl2−0.2% Et3N), m/z obs=430 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07923466B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-42f3d3f7fb85493e98d97fe288895345 |
| Source note | uspto-grants-2011_04 |