HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butoxy bis(dimethylamino)methane → 6-[1-Dimethylamino-methylidene]-2-(2,4-dichloro-phenyl)-cyclohexanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butoxy bis(dimethylamino)methane | HCID 79885 | — |
| Reactant | 2-(2,4-Dichlorophenyl)cyclohexan-1-one | HCID 18441761 | — |
| Product | 6-[1-Dimethylamino-methylidene]-2-(2,4-dichloro-phenyl)-cyclohexanone | HCID 67096111 | — |
Reaction Steps
2-(2,4-dichloro-phenyl)-cyclohexanone (101 mg, 0.42 mmol) was reacted with tert.-butoxy-bis-(dimethylamino)-methane using in analogous manner the procedure described in example 45a) to give crude title compound (105 mg) as a red oil which was used directly in the next step. MS ISP (m/e): 298.3 [(M+H)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07923450B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-9be76db7ba004c96a6d8787a8d385ae2 |
| Source note | uspto-grants-2011_04 |