HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butoxy bis(dimethylamino)methane → HCID 67096159, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butoxy bis(dimethylamino)methane | HCID 79885 | — |
| Reactant | HCID 62800456 | HCID 62800456 | — |
| Product | HCID 67096159 | HCID 67096159 | — |
Reaction Steps
2-(2,5-Dichloro-phenyl)-cycloheptanone (157 mg, 0.61 mmol) was reacted with tert.-butoxy-bis-(dimethylamino)-methane using in analogous manner the procedure described in example 45a) to give crude title compound (197 mg) as a red solid which was used directly in the next step. MS ISP (m/e): 312.0 [(M+H)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07923450B2 |
| Source dataset | uspto-grants-2011_04 |
| ORD ID | ord-7bff43b4dcdb4c5e9e6a61b54a9d810c |
| Source note | uspto-grants-2011_04 |